(R)-(+)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl CAS NO.76189-55-4

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(R)-(+)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl CAS NO.76189-55-4
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MF:C44H32P2
MW:622.69
EINECS:616-304-7
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(R)-(+)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl Basic information

Product Name (R)-(+)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl
Synonyms (R)-(+)-BINAP, (R)-(+)-1,1'-Binaphthalene-2,2'-diylbis(diphenylphosphane);(R)-(+)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthalene 97%;(R)-(+)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl;R(+)-2,2'-BIS(DIPHENYLPHOSPHINO)-1,1'-BINAPHTHALENE;(R)-(+)-2,2'-BIS(DIPHENYLPHOSPHINO)-1,1'-BINAPHTHYL;(R)-(+)-2,2BIS(DIPHENYLPHOSPHINO)-1,1-BINAPHTHYL;(R)-2,2'-BIS(DIPHENYLPHOSPHINO)-1,1'-BINAPHTHYL;(R)-(+)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl,(R)-BINAP
CAS 76189-55-4
MF C44H32P2
MW 622.69
EINECS 616-304-7

 

(R)-(+)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl Chemical Properties

Melting point 283-286 °C(lit.)
alpha 240 º (c=0.3, toluene)
Boiling point 724.3±55.0 °C(Predicted)
refractive index 235 ° (C=0.3, Toluene)
storage temp. Inert atmosphere,Room Temperature
solubility Benzene (Slightly), Chloroform (Slightly)
form Powder
color White to cream-white
optical activity [α]20/D +222°, c = 0.5% in benzene
Water Solubility insoluble
Sensitive Air Sensitive

 

(R)-(+)-2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl Usage And Synthesis

Chemical Properties white to light yellow crystal powde
Uses Useful ligand for transition metal catalyzed asymmetric reactions, including hydrogenation and disilylation. 2,2′-Bis(diphenylphosphino)-1,1′-binaphthyl and its rhodium and ruthenium derivatives are highly selective homogeneous catalysts used for the reduction of aryl ketones, β-keto esters, and α-amino ketones. They have also been used for asymmetric hydrogenation and hydroformylation of olefins, asymmetric Heck reactions, and asymmetric isomerizations of allyls.
Complex with Ag(I) used to catalyze an asymmetric aldol reaction between alkenyl trichloroacetates and aldehydes. Also used with Ag(I) to catalyze an enantioselective hetero-Diels-Alder reaction of azo compounds.
General Description (R)-(+)-2,2′-Bis(diphenylphosphino)-1,1′-binaphthalene is an axially dissymmetric bis(triaryl)phosphine ligand for asymmetric reactions.

 

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